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The pressure/temperature phase diagram of LiAlH₄ has been constructed by using Raman spectroscopy data. In situ high pressureâˆ’temperature experiments were carried out using resistively heated diamond anvil cells up to 150 Â°C and 7 GPa. Room temperature phase transitions of monoclinic Î±-LiAlH₄ â†’ Î´-LiAlH₄ were observed at ~3.2 GPa. As the temperature is increased to ~100 Â°C, both the Î± and Î´ phases transform to Î²-LiAlH₄ and remain stable up to 5.5 GPa. At temperatures greater than 300 Â°C, a new Î³-LiAlH₄ phase forms. Data of Konovalov (1995) has been used to define the phase boundary between Î²- and Î³-LiAlH₄ phases. We present a pressureâˆ’temperature phase diagram of LiAlH₄ based using diamond anvil cells coupled with Raman spectroscopy.

Raman Spectroscopy Measurements of the Pressure−Temperature Behavior of LiAlH₄ J.C. Fallas, W.-M. Chien, D. Chandra, V.K. Kamisetty, E.D. Emmons, A.M. Covington, R. Chellappa, S.A. Gramsch, R.J. Hemley and H. Hagemann Journal of Physical Chemistry C, 114 (27) (2010), p11991-11997 DOI:10.1021/jp1015017 \| unige:14747 \| Abstract \| Article HTML \| Article PDF
The pressure/temperature phase diagram of LiAlH₄ has been constructed by using Raman spectroscopy data. In situ high pressureâˆ’temperature experiments were carried out using resistively heated diamond anvil cells up to 150 Â°C and 7 GPa. Room temperature phase transitions of monoclinic Î±-LiAlH₄ â†’ Î´-LiAlH₄ were observed at ~3.2 GPa. As the temperature is increased to ~100 Â°C, both the Î± and Î´ phases transform to Î²-LiAlH₄ and remain stable up to 5.5 GPa. At temperatures greater than 300 Â°C, a new Î³-LiAlH₄ phase forms. Data of Konovalov (1995) has been used to define the phase boundary between Î²- and Î³-LiAlH₄ phases. We present a pressureâˆ’temperature phase diagram of LiAlH₄ based using diamond anvil cells coupled with Raman spectroscopy.

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